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Gold in iron ore samples is separated from iron (major matrix cation), antimony and vanadium using anion exchange resin in (0.2 M) HBr, potassium peroxodisulfate and acetone:water:nitric acid media. The exchangeable anion Cl − of the ion exchanger Dowex 1X 4 is replaced by Br − using (6 M) HBr solution.
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